Difference between revisions of "Minutes-8-23-2012"

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= Agenda =
 
= Agenda =
 +
# Production [http://www.jlab.org/Hall-D/detector/fdc/production/FDC_Construction_August_23_2012.xlsx Construction Tracking] (Dave)
 +
#* Cathodes
 +
#* Third package
 
# Cathode corrosion
 
# Cathode corrosion
#* Status [http://www.jlab.org/Hall-D/detector/fdc/corrosion/2012-08-03-09.40.08.jpg tests with water], [http://www.jlab.org/Hall-D/detector/fdc/corrosion/EPDM-Viton-water-08-06-12 SEM results]
+
#* Results from SEM analyses: [http://www.jlab.org/Hall-D/detector/fdc/corrosion/]
#* Testing chambers [http://www.jlab.org/Hall-D/detector/fdc/corrosion/2012-08-09-10.27.32.jpg vacuum chamber tests]
+
#* Test chambers  
# Production [http://www.jlab.org/Hall-D/detector/fdc/production/FDC_Construction_August_9_2012.xlsx Construction Tracking] (Dave)
+
# Engineering (Dave)
#* Cathode production
+
#* Cathode strong-backs
#* Fixing cathodes
+
#* Second package refurbishment
+
# Engineering (Bill)
+
 
# Electronics (Chris, Nick)
 
# Electronics (Chris, Nick)
# [http://www.jlab.org/Hall-D/detector/fdc/general/tdr.pdf TDR, page 132-145] (Lubomir)
+
#* PCBs
 +
# [http://www.jlab.org/Hall-D/detector/fdc/general/tdr.pdf TDR, pages 132-145] (Lubomir)
 
# Other
 
# Other
 
<!--
 
  
 
= Minutes =
 
= Minutes =
  
Participants: Bill, Dave, Chris, Nick, Vlad, Eugene, and Lubomir
+
Participants: Fernando, Tim, Eugene, Dave, Simon, Vlad, and Lubomir
  
 +
== Production ==
  
== Cathode corrosion ==
+
- Dave: working on 10 new cathodes to be used in the first package, not in the second package as we always stated before. Again the bottleneck is the card gluing, but we will start making progress there, by tomorrow we plan to have the cathode strong-backs ready to be used to move the cathodes. Will start working soon on the other two cathodes that are needed to finish the first package. After that we will have two sets of cathode foils left.
  
- Lubomir: a test with cathode foils, Viton/EPDM O-rings and water was done (at Blue Crab dirty area). First, the O-ring samples were pressed against the foils with a lead brick, also using G10 and aluminum plates to equalize the pressure. After a couple of days, water (from the tab) was put on the samples. Corrosion appeared immediately on the next day: very well pronounced on the EPDM sample and resembling the same dark traces that we had on the cathodes of the first and second packages (see first picture above), also some corrosion but with lighter color on the Viton sample. Olga did SEM analyses on the two sample foils at the places of the O-rings: second link above. Generally, the experiment was not done in a clean environment and tab water was used, so you see a lot of dirty  stuff like chlorine. At the same time sulfur is visible in almost all the areas of the EPDM sample, while for the Viton sample sulfur is present in much smaller areas visible with high magnification. We started the same experiment inside the clean room using distilled water; expect results next week.
+
- The third package is ready with the subsystems: grounding, cooling tubes, HV cabling. The plan is to move it to 126 tomorrow. The grounding worked fine, Vlad put ~100 clips for grounding as planned and another ~100 attached close to both sides of the cards (where possible and needed) to prevent the cathode deformation at the periphery. As Casey suggested, we used a new method to install the cooling tubes. We tightened the bracket on one card in the middle of the tube and installed the rest of the brackets loose. Then, going from the middle card toward the two ends of the tube we tightened the rest of the brackets. Thus, the copper tubes apply some pressure on the cards; before we had problems with some of the cards being pulled by the tubes. Gluing of the back brackets with green epoxy to the tubes was done at the end. In 126 after installing the cables we should experiment how easy will be to remove the extra clips we put on the card sides.
  
- Three other test experiments are running. One with production cathodes and a wire frame that started more than two weeks ago. Second one with similar samples using the small-scale prototype, running since yesterday when we were able to fix the HV. The third one is the Vlad's experiment using the vacuum chamber (picture linked) with same samples (EPDM, Viton with/without Apiezon) with same gas, but no HV, with some water inside to create moisture, all this heated with a lamp (only during the day) up to 80degC. It started yesterday; we will open the chamber on Monday.
+
== Cathode corrosion ==
  
== Production ==
+
- New SEM results from Olga (follow the above link) for the samples from the Vlad's test with the vacuum chamber; the chamber had water inside and the temperature at end of the day (lamps were off overnight) was close to 100degC.  The test was done for about 4 days:
  
- Dave: cathode #61 (type-3) that was supposed to be the first for package #2 showed a problem: the Mylar peeled off on the second day after gluing it. The surface is tacky. Bill will consult with the manufacturer of the Hysol epoxy and we will do several experiments to test it. The frame was re-used, Casey sanded it with #220 as he did for the frames that were converted to type-2 from type-1, but using different sanding tool. Tomorrow we will see if the surface will be still tacky and will re-sand it in the same way as for the converted frames.  
+
*Copper foil with EPDM inside: significant corrosion, a lot of sulfur present.
 +
 +
*With the EPDM of the gasket, part of the foil strips were inside the gas chamber and part exposed to the air: no sulfur seen at the air side and a lot of it at the gas side. However, inside the gas volume there was moisture and the temperature was much higher than outside. We had seen corrosion before also in the samples placed in air with some water put on the foils and no heating. We will do more tests.  
  
- We discussed the change/instability of the resistance of the cathode contacts (present for several percents of the total number of channels). We measure the resistances every time we put a cathode in the stack. It is more prominent for the older cathodes and we are not sure if it is a results of some kind of aging, or simply due to more handling and deforming of the cathode frames. Vlad is looking if the bad channels are just statistical fluctuation. Looking with a microscope on the conductive tape he counted that we have ~76 silver balls per pad (2.5x0.5 mm^2), but only ~20 of them are big. Assuming Poisson distribution, in about few percents of the contacts one could expect a resistance that is twice bigger than the mean one. Vlad will do measurements of the resistance of the contacts on one (or more) cathode to see if it can be explained just statistically.  
+
*Copper foil with Viton: some traces visible, almost no sulfur there but some chlorine. Tim suggested cleaning the O-rings before installation.  
  
- Most likely the z-axis conductive tape technology will be a concern for the coming few years, therefore we discussed the conventional way of soldering to the 2micron copper. Anatoly and Casey soldered two connectors successfully, the question is what is the yield. Bill: according to Mark one has to control the heat on the copper very well, he has seen melting the copper. Another important question is, what if for example one has to replace a broken connector on the daughter-card. Unlike with the conductive tape technology, un-soldering the rigid-flex is not possible. Anatoly tried it; the only way one can do it is by cutting the flex channel by channel but then there's a good chance to cut part of the copper traces. Eugene: can we replace the connector while the daughter card is on the cathode. Chris and Dave will try to test if that's possible. Certainly these discussions will continue.
+
*With Viton and Apiezon: no visible corrosion, only copper and carbon lines are visible, but the grease was not cleaned. Olga will repeat the measurements after cleaning it.  
  
- Cathode #2 (type-3), one of the first cathodes, showed high resistance on some of the channels in two connectors, in total 8-10 channels, that could not be fixed. We decided to try to fix these channels by soldering a wire between the top of the flex pad and the copper trace just outside of the spacer ring (we have about 3mm trace there), as Anatoly suggested. Anatoly and Chris will give it a try.
+
- The first testing chamber with production wire frame and cathodes was opened yesterday, exactly 4 weeks operating with HV and gas. Some traces from the EPDM O-ring are visible but it doesn't look like the corrosion on the first and second packages. We conclude that the humidity is an important factor. No traces on the cathode against the Viton+Apiezon O-ring are visible. The test with the small-scale prototype is running two weeks, haven't opened it yet.
  
- We decided to continue with the above tests and postpone for one more week the installation of the second package. We are flushing the third and the fourth packages (in parallel) with nitrogen since last Friday when we got a dewar.  
+
- Tim for the humidity conditions in the Hall: nominally it will be less than 45%, but he can't exclude some periods when it might be higher. There will be dry air blowing through the magnet. We should avoid opening the Hall doors for a long time during the installation.
  
 
== Engineering ==
 
== Engineering ==
  
- Bill will work on designing a tool for the cathodes to keep them flat during the installation. He made one some time ago that works with vacuum, but it can be used only at one side of the cathode.  
+
- We will have two strong-backs to be used to grab the cathodes from both sides and keep them flat. We discussed how to support the cathode periphery when using the strong-backs. Casey made a table with rods that will be used to store the cathodes in a flat position.
  
 +
- The rings for the cathode strong-backs came from the REX company right after the meeting, but there were issues with the fittings for the suction cups; also the weight of the aluminum ring seams too big.
 +
 
== Electronics ==
 
== Electronics ==
  
- Roger talked to Allflex, they will find out how much material we have there. Roger will ask for quotation but we have to decide for how many foil sets. Eugene proposed to have two options: 1) the minimum, which is 20 sets (if we are to replace all the cathodes from the first two packages, i.e. 24, and we have 14 spares we will need 10 more sets, plus 10 spares) or 2) 50 sets which close to the total material there.
+
- Fernando: wrong zip file was send to the company for the PCBs; now all the files have the correct names to exclude such a problem.  
  
- According to Dave we can re-use a high percentage of the old daughter cards (rigid-flex assemblies), therefore we will ask for a quotation only for 20 cathodes, times 9 cards on each: ~200 cards.
+
- Main discussion was what to do the with these four PCB sets. Mechanically, compared to the original PCBs, there is a small difference in the gas connector positions (about a mm); according to Tim it will work and mechanically the wire planes will be interchangeable. Fernando: some of the signal traces are at different positions and the gold-plated ground area is bigger; the traces going through that area have to be covered with conformal coating. There should be no differences in the HV PCBs, but Fernando will check all the boards and on Monday we will decide if these can be used. Eugene: if you spend more than two weeks on these boards we better purchase new ones, which however will be tricky (at the end of the fiscal year) and will delay the production. Lubomir and Dave: we will need the boards in two weeks, if not we have to re-work the schedule.
  
 
== TDR ==
 
== TDR ==
  
- Lubomir added few subsections in the TDR, we should have a preliminary version for the next meeting.
+
- Lubomir received corrections from Bill and Simon, still some work remains to be done here.
 +
 
 +
== Other ==
  
-->
+
- Eugene urges us to do all the purchases for the FDC as soon as possible at least by the beginning of September; after that most likely there will be no money till the end of FY12.

Latest revision as of 16:35, 24 August 2012

August 23, 2012 FDC meeting

Agenda

  1. Production Construction Tracking (Dave)
    • Cathodes
    • Third package
  2. Cathode corrosion
    • Results from SEM analyses: [1]
    • Test chambers
  3. Engineering (Dave)
    • Cathode strong-backs
  4. Electronics (Chris, Nick)
    • PCBs
  5. TDR, pages 132-145 (Lubomir)
  6. Other

Minutes

Participants: Fernando, Tim, Eugene, Dave, Simon, Vlad, and Lubomir

Production

- Dave: working on 10 new cathodes to be used in the first package, not in the second package as we always stated before. Again the bottleneck is the card gluing, but we will start making progress there, by tomorrow we plan to have the cathode strong-backs ready to be used to move the cathodes. Will start working soon on the other two cathodes that are needed to finish the first package. After that we will have two sets of cathode foils left.

- The third package is ready with the subsystems: grounding, cooling tubes, HV cabling. The plan is to move it to 126 tomorrow. The grounding worked fine, Vlad put ~100 clips for grounding as planned and another ~100 attached close to both sides of the cards (where possible and needed) to prevent the cathode deformation at the periphery. As Casey suggested, we used a new method to install the cooling tubes. We tightened the bracket on one card in the middle of the tube and installed the rest of the brackets loose. Then, going from the middle card toward the two ends of the tube we tightened the rest of the brackets. Thus, the copper tubes apply some pressure on the cards; before we had problems with some of the cards being pulled by the tubes. Gluing of the back brackets with green epoxy to the tubes was done at the end. In 126 after installing the cables we should experiment how easy will be to remove the extra clips we put on the card sides.

Cathode corrosion

- New SEM results from Olga (follow the above link) for the samples from the Vlad's test with the vacuum chamber; the chamber had water inside and the temperature at end of the day (lamps were off overnight) was close to 100degC. The test was done for about 4 days:

  • Copper foil with EPDM inside: significant corrosion, a lot of sulfur present.
  • With the EPDM of the gasket, part of the foil strips were inside the gas chamber and part exposed to the air: no sulfur seen at the air side and a lot of it at the gas side. However, inside the gas volume there was moisture and the temperature was much higher than outside. We had seen corrosion before also in the samples placed in air with some water put on the foils and no heating. We will do more tests.
  • Copper foil with Viton: some traces visible, almost no sulfur there but some chlorine. Tim suggested cleaning the O-rings before installation.
  • With Viton and Apiezon: no visible corrosion, only copper and carbon lines are visible, but the grease was not cleaned. Olga will repeat the measurements after cleaning it.

- The first testing chamber with production wire frame and cathodes was opened yesterday, exactly 4 weeks operating with HV and gas. Some traces from the EPDM O-ring are visible but it doesn't look like the corrosion on the first and second packages. We conclude that the humidity is an important factor. No traces on the cathode against the Viton+Apiezon O-ring are visible. The test with the small-scale prototype is running two weeks, haven't opened it yet.

- Tim for the humidity conditions in the Hall: nominally it will be less than 45%, but he can't exclude some periods when it might be higher. There will be dry air blowing through the magnet. We should avoid opening the Hall doors for a long time during the installation.

Engineering

- We will have two strong-backs to be used to grab the cathodes from both sides and keep them flat. We discussed how to support the cathode periphery when using the strong-backs. Casey made a table with rods that will be used to store the cathodes in a flat position.

- The rings for the cathode strong-backs came from the REX company right after the meeting, but there were issues with the fittings for the suction cups; also the weight of the aluminum ring seams too big.

Electronics

- Fernando: wrong zip file was send to the company for the PCBs; now all the files have the correct names to exclude such a problem.

- Main discussion was what to do the with these four PCB sets. Mechanically, compared to the original PCBs, there is a small difference in the gas connector positions (about a mm); according to Tim it will work and mechanically the wire planes will be interchangeable. Fernando: some of the signal traces are at different positions and the gold-plated ground area is bigger; the traces going through that area have to be covered with conformal coating. There should be no differences in the HV PCBs, but Fernando will check all the boards and on Monday we will decide if these can be used. Eugene: if you spend more than two weeks on these boards we better purchase new ones, which however will be tricky (at the end of the fiscal year) and will delay the production. Lubomir and Dave: we will need the boards in two weeks, if not we have to re-work the schedule.

TDR

- Lubomir received corrections from Bill and Simon, still some work remains to be done here.

Other

- Eugene urges us to do all the purchases for the FDC as soon as possible at least by the beginning of September; after that most likely there will be no money till the end of FY12.